TA Instruments

AR1705-0001f

04/09/2012 16:19:28

Sample name	ASW 10 mm from base, 60 mm to top, disk 18 PMMA+FA fouled
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1705
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 16:19:28

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-9.818	7.690	-1.277	1.0080	22.4	-160.4	5.3474	10000	-0.03936	-2.712	6.6842	668.42	3.384E-3	0.0	1.0	61.008	-30.121	6.152
0.7714	12.22	0.06315	2.0240	22.4	-155.4	13.0741	10000	-0.03814	-1.042	16.343	1634.3	3.384E-3	0.0	1.0	62.024	2.3667	9.772
1.510	19.31	0.07818	3.0080	22.4	-148.8	26.7750	10000	-0.03652	-0.3991	33.469	3346.9	3.384E-3	0.1	1.1	63.008	4.6314	15.45
2.110	23.00	0.09175	4.0040	22.4	-149.6	40.7291	10000	-0.03672	-0.2829	50.911	5091.1	3.384E-3	0.1	1.1	64.004	6.4737	18.40
3.492	30.82	0.1133	5.0120	22.4	-146.3	67.5044	10000	-0.03591	-0.1540	84.381	8438.1	3.384E-3	0.1	1.1	65.012	10.713	24.66
5.375	39.47	0.1362	6.0080	22.4	-162.9	106.5740	10000	-0.03997	-0.1045	133.22	13322	3.384E-3	0.1	1.1	66.008	16.490	31.58
5.985	42.52	0.1407	7.0080	22.4	-146.3	126.4520	10000	-0.03591	-0.08092	158.07	15807	3.384E-3	0.1	1.1	67.008	18.362	34.02
7.553	49.12	0.1538	8.0080	22.4	-165.3	165.6840	10000	-0.04058	-0.06853	207.11	20711	3.384E-3	0.1	1.1	68.008	23.171	39.29
9.961	57.52	0.1732	9.0240	22.4	-167.0	223.0180	10000	-0.04098	-0.05047	278.77	27877	3.384E-3	0.2	1.2	69.024	30.560	46.02
11.91	62.87	0.1895	10.008	22.4	-173.6	268.0340	10000	-0.04261	-0.04392	335.04	33504	3.384E-3	0.2	1.2	70.008	36.545	50.30
13.71	68.91	0.1990	11.008	22.4	-168.6	319.3540	10000	-0.04139	-0.03552	399.19	39919	3.384E-3	0.2	1.2	71.008	42.067	55.13
15.57	74.43	0.2092	12.008	22.4	-183.5	370.5420	10000	-0.04504	-0.03313	463.18	46318	3.384E-3	0.2	1.2	72.008	47.764	59.54
18.16	82.30	0.2206	13.028	22.4	-168.6	453.5270	10000	-0.04139	-0.02490	566.91	56691	3.383E-3	0.2	1.2	73.028	55.706	65.84
20.45	88.09	0.2321	14.024	22.4	-175.3	517.3710	10000	-0.04301	-0.02258	646.71	64671	3.384E-3	0.2	1.2	74.024	62.742	70.48
22.60	93.53	0.2416	15.024	22.4	-183.5	581.0980	10000	-0.04504	-0.02098	726.37	72637	3.384E-3	0.3	1.3	75.024	69.329	74.82
26.05	101.3	0.2570	16.024	22.4	-189.3	682.9240	10000	-0.04646	-0.01843	853.66	85366	3.384E-3	0.3	1.3	76.024	79.918	81.08
28.05	107.0	0.2621	17.024	22.4	-195.1	759.2720	10000	-0.04788	-0.01703	949.09	94909	3.384E-3	0.3	1.3	77.024	86.071	85.62
30.35	112.4	0.2700	18.024	22.4	-195.1	835.5730	10000	-0.04788	-0.01544	1044.5	1.0445E5	3.384E-3	0.3	1.3	78.024	93.104	89.92
32.53	117.5	0.2768	19.008	22.4	-189.3	911.8070	10000	-0.04646	-0.01371	1139.8	1.1398E5	3.384E-3	0.3	1.3	79.008	99.791	94.02
36.58	125.8	0.2908	20.008	22.4	-202.5	1045.1000	10000	-0.04971	-0.01280	1306.4	1.3064E5	3.383E-3	0.3	1.3	80.008	112.24	100.6
39.16	131.1	0.2986	21.024	22.4	-217.4	1133.9700	10000	-0.05336	-0.01264	1417.5	1.4175E5	3.383E-3	0.4	1.4	81.024	120.14	104.9
41.78	136.3	0.3066	22.024	22.4	-210.0	1222.6801	10000	-0.05153	-0.01131	1528.4	1.5284E5	3.383E-3	0.4	1.4	82.024	128.17	109.0
45.23	144.5	0.3130	23.024	22.4	-205.8	1375.4399	10000	-0.05052	-9.860E-3	1719.3	1.7193E5	3.384E-3	0.4	1.4	83.024	138.76	115.6
47.93	149.8	0.3199	24.024	22.4	-218.2	1476.2500	10000	-0.05356	-9.723E-3	1845.3	1.8453E5	3.384E-3	0.4	1.4	84.024	147.06	119.9
50.40	155.0	0.3252	25.004	22.4	-224.8	1578.0699	10000	-0.05519	-9.364E-3	1972.6	1.9726E5	3.384E-3	0.4	1.4	85.004	154.62	124.0
54.71	162.8	0.3360	26.028	22.4	-226.5	1742.2500	10000	-0.05559	-8.544E-3	2177.8	2.1778E5	3.384E-3	0.4	1.4	86.028	167.83	130.3
57.68	168.1	0.3431	27.024	22.4	-224.8	1856.2000	10000	-0.05519	-7.953E-3	2320.3	2.3203E5	3.384E-3	0.5	1.5	87.024	176.97	134.5
62.44	175.8	0.3551	28.028	22.4	-221.5	2026.9500	10000	-0.05437	-7.167E-3	2533.7	2.5337E5	3.384E-3	0.5	1.5	88.028	191.55	140.7
65.78	181.2	0.3631	29.024	22.4	-230.6	2153.5801	10000	-0.05661	-7.027E-3	2692.0	2.6920E5	3.384E-3	0.5	1.5	89.024	201.82	144.9
68.95	186.5	0.3697	30.024	22.4	-240.6	2280.0801	10000	-0.05904	-6.917E-3	2850.1	2.8501E5	3.384E-3	0.5	1.5	90.024	211.53	149.2
73.44	194.2	0.3782	31.024	22.4	-253.8	2469.7000	10000	-0.06229	-6.730E-3	3087.1	3.0871E5	3.384E-3	0.5	1.5	91.024	225.31	155.4
76.42	199.3	0.3835	32.024	22.4	-238.1	2603.1101	10000	-0.05843	-5.995E-3	3253.9	3.2539E5	3.384E-3	0.5	1.5	92.024	234.46	159.4
79.83	204.6	0.3901	33.024	22.4	-242.2	2741.6299	10000	-0.05945	-5.785E-3	3427.0	3.4270E5	3.383E-3	0.6	1.6	93.024	244.90	163.7
84.12	212.3	0.3961	34.024	22.4	-231.5	2950.2400	10000	-0.05681	-5.133E-3	3687.8	3.6878E5	3.384E-3	0.6	1.6	94.024	258.07	169.9
87.60	217.5	0.4028	35.032	22.4	-241.4	3095.3999	10000	-0.05924	-5.104E-3	3869.3	3.8693E5	3.383E-3	0.6	1.6	95.032	268.75	174.0
91.73	222.8	0.4117	36.024	22.4	-248.8	3247.4800	10000	-0.06107	-5.013E-3	4059.4	4.0594E5	3.384E-3	0.6	1.6	96.024	281.41	178.2
96.93	230.6	0.4204	37.024	22.4	-263.7	3474.3601	10000	-0.06472	-4.961E-3	4343.0	4.3430E5	3.384E-3	0.6	1.6	97.024	297.39	184.4
100.3	235.6	0.4256	38.072	22.4	-266.2	3625.9700	10000	-0.06533	-4.797E-3	4532.5	4.5325E5	3.384E-3	0.6	1.6	98.072	307.62	188.5
105.3	243.4	0.4325	39.024	22.4	-267.8	3873.0601	10000	-0.06574	-4.520E-3	4841.3	4.8413E5	3.384E-3	0.7	1.7	99.024	322.97	194.7
108.8	248.6	0.4377	40.012	22.4	-267.0	4036.3899	10000	-0.06553	-4.321E-3	5045.5	5.0455E5	3.384E-3	0.7	1.7	100.012	333.83	198.9
115.1	256.1	0.4492	41.024	22.4	-265.4	4287.2798	10000	-0.06513	-4.045E-3	5359.1	5.3591E5	3.384E-3	0.7	1.7	101.024	352.98	204.9
118.4	261.3	0.4529	42.024	22.4	-270.3	4459.3701	10000	-0.06635	-3.958E-3	5574.2	5.5742E5	3.384E-3	0.7	1.7	102.024	363.13	209.1
122.6	266.5	0.4600	43.008	22.4	-267.8	4636.1802	10000	-0.06574	-3.771E-3	5795.2	5.7952E5	3.384E-3	0.7	1.7	103.008	376.10	213.2
127.5	274.1	0.4651	44.024	22.4	-286.0	4901.1602	10000	-0.07020	-3.808E-3	6126.5	6.1265E5	3.384E-3	0.7	1.7	104.024	391.11	219.3
133.9	281.9	0.4749	45.344	22.4	-287.7	5185.1201	10000	-0.07061	-3.620E-3	6481.4	6.4814E5	3.383E-3	0.8	1.8	105.344	410.74	225.5
137.3	287.1	0.4784	46.024	22.4	-287.7	5376.2300	10000	-0.07061	-3.491E-3	6720.3	6.7203E5	3.383E-3	0.8	1.8	106.024	421.33	229.6
140.7	292.1	0.4817	47.004	22.4	-305.0	5563.6699	10000	-0.07487	-3.575E-3	6954.6	6.9546E5	3.384E-3	0.8	1.8	107.004	431.63	233.7
145.2	297.2	0.4886	48.024	22.4	-319.9	5760.3999	10000	-0.07852	-3.623E-3	7200.5	7.2005E5	3.384E-3	0.8	1.8	108.024	445.43	237.7
151.7	304.9	0.4975	49.056	22.4	-305.0	6062.0200	10000	-0.07487	-3.281E-3	7577.5	7.5775E5	3.384E-3	0.8	1.8	109.056	465.45	243.9
155.9	310.0	0.5030	50.032	22.4	-326.5	6266.0400	10000	-0.08014	-3.398E-3	7832.6	7.8326E5	3.383E-3	0.8	1.8	110.032	478.40	248.0
159.3	317.5	0.5018	51.024	22.4	-320.7	6576.7500	10000	-0.07872	-3.181E-3	8220.9	8.2209E5	3.384E-3	0.9	1.9	111.024	488.88	254.0
165.1	322.7	0.5115	52.024	22.4	-342.2	6787.3999	10000	-0.08400	-3.286E-3	8484.3	8.4843E5	3.384E-3	0.9	1.9	112.024	506.41	258.2
173.9	330.3	0.5264	53.024	22.4	-343.1	7110.5601	10000	-0.08420	-3.144E-3	8888.2	8.8882E5	3.384E-3	0.9	1.9	113.024	533.52	264.3
176.5	335.4	0.5263	54.008	22.4	-345.5	7329.8799	10000	-0.08481	-3.071E-3	9162.4	9.1624E5	3.383E-3	0.9	1.9	114.008	541.59	268.3
179.3	340.6	0.5264	55.008	22.4	-348.0	7559.9600	10000	-0.08542	-3.000E-3	9450.0	9.4500E5	3.383E-3	0.9	1.9	115.008	550.07	272.5
186.2	348.2	0.5347	56.028	22.4	-357.9	7897.4399	10000	-0.08785	-2.952E-3	9871.8	9.8718E5	3.383E-3	0.9	1.9	116.028	571.24	278.6
192.6	353.2	0.5452	57.024	22.4	-351.3	8124.2100	10000	-0.08623	-2.816E-3	10155	1.0155E6	3.383E-3	1.0	2.0	117.024	590.85	282.6
198.6	361.0	0.5501	58.024	22.4	-324.9	8483.6201	10000	-0.07974	-2.493E-3	10605	1.0605E6	3.384E-3	1.0	2.0	118.024	609.19	288.8
201.6	366.1	0.5507	59.008	22.4	-328.2	8723.1699	10000	-0.08055	-2.449E-3	10904	1.0904E6	3.383E-3	1.0	2.0	119.008	618.40	292.8
208.8	373.6	0.5588	60.028	22.4	-365.4	9082.4297	10000	-0.08968	-2.618E-3	11353	1.1353E6	3.383E-3	1.0	2.0	120.028	640.44	298.9

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

212.2	375.0	0.5659	1.0040	22.4	-366.2	244.9740	10000	-0.08988	-2.604E-3	306.22	30622	3.383E-3	0.0	2.0	122.004	651.07	300.0
212.3	375.0	0.5662	2.0200	22.4	-381.9	621.9580	10000	-0.09374	-2.716E-3	777.45	77745	3.384E-3	0.0	2.1	123.020	651.43	300.0
215.2	375.0	0.5737	3.0200	22.4	-382.7	873.4580	10000	-0.09394	-2.722E-3	1091.8	1.0918E5	3.384E-3	0.1	2.1	124.020	660.07	300.0
213.6	375.0	0.5695	4.0200	22.4	-375.3	1124.6300	10000	-0.09211	-2.669E-3	1405.8	1.4058E5	3.384E-3	0.1	2.1	125.020	655.22	300.0
212.3	375.0	0.5661	5.0240	22.4	-381.1	1501.8800	10000	-0.09353	-2.710E-3	1877.4	1.8774E5	3.383E-3	0.1	2.1	126.024	651.32	300.0
211.6	375.0	0.5643	6.0200	22.4	-404.2	1753.0900	10000	-0.09921	-2.874E-3	2191.4	2.1914E5	3.384E-3	0.1	2.1	127.020	649.25	300.0
215.6	375.0	0.5749	7.0200	22.4	-392.7	2132.0601	10000	-0.09637	-2.792E-3	2665.1	2.6651E5	3.383E-3	0.1	2.1	128.020	661.44	300.0
211.9	375.0	0.5650	8.0200	22.4	-348.0	2381.2000	10000	-0.08542	-2.475E-3	2976.5	2.9765E5	3.384E-3	0.1	2.2	129.020	650.07	300.0
213.2	375.0	0.5685	9.0200	22.4	-386.0	2632.7400	10000	-0.09475	-2.745E-3	3290.9	3.2909E5	3.383E-3	0.2	2.2	130.020	654.09	300.0
214.3	375.0	0.5716	10.024	22.4	-391.8	3009.7100	10000	-0.09617	-2.786E-3	3762.1	3.7621E5	3.384E-3	0.2	2.2	131.024	657.58	300.0
211.1	375.0	0.5629	11.020	22.4	-388.5	3266.2800	10000	-0.09536	-2.763E-3	4082.9	4.0829E5	3.384E-3	0.2	2.2	132.020	647.57	300.0
210.7	375.0	0.5619	12.020	22.4	-371.2	3512.3301	10000	-0.09110	-2.639E-3	4390.4	4.3904E5	3.384E-3	0.2	2.2	133.020	646.51	300.0
213.3	375.0	0.5687	13.020	22.4	-397.6	3889.3201	10000	-0.09759	-2.827E-3	4861.7	4.8617E5	3.384E-3	0.2	2.2	134.020	654.29	300.0
213.8	375.0	0.5700	14.020	22.4	-377.0	4140.7998	10000	-0.09252	-2.681E-3	5176.0	5.1760E5	3.384E-3	0.2	2.3	135.020	655.78	300.0
212.5	375.0	0.5666	15.024	22.4	-355.5	4517.6401	10000	-0.08724	-2.528E-3	5647.1	5.6471E5	3.384E-3	0.3	2.3	136.024	651.87	300.0
214.5	375.0	0.5719	16.020	22.4	-380.3	4768.9502	10000	-0.09333	-2.704E-3	5961.2	5.9612E5	3.384E-3	0.3	2.3	137.020	658.02	300.0
211.8	375.0	0.5648	17.020	22.4	-351.3	5020.4102	10000	-0.08623	-2.498E-3	6275.5	6.2755E5	3.384E-3	0.3	2.3	138.020	649.82	300.0
214.2	375.0	0.5712	18.024	22.4	-399.3	5397.2900	10000	-0.09800	-2.839E-3	6746.6	6.7466E5	3.383E-3	0.3	2.3	139.024	657.12	300.0
212.4	375.0	0.5665	19.020	22.4	-386.9	5649.8799	10000	-0.09495	-2.751E-3	7062.4	7.0624E5	3.384E-3	0.3	2.3	140.020	651.73	300.0
213.8	375.0	0.5702	20.020	22.4	-385.2	6028.3101	10000	-0.09455	-2.739E-3	7535.4	7.5354E5	3.383E-3	0.3	2.4	141.020	655.95	300.0
213.5	375.0	0.5693	21.020	22.4	-360.4	6276.8198	10000	-0.08846	-2.563E-3	7846.0	7.8460E5	3.384E-3	0.4	2.4	142.020	654.99	300.0
213.3	375.0	0.5688	22.020	22.4	-359.6	6529.5498	10000	-0.08826	-2.557E-3	8161.9	8.1619E5	3.384E-3	0.4	2.4	143.020	654.42	300.0
212.3	375.0	0.5661	23.020	22.4	-407.5	6905.4902	10000	-0.1000	-2.898E-3	8631.9	8.6319E5	3.384E-3	0.4	2.4	144.020	651.31	300.0
210.6	375.0	0.5617	24.024	22.4	-361.2	7158.5601	10000	-0.08866	-2.569E-3	8948.2	8.9482E5	3.383E-3	0.4	2.4	145.024	646.26	300.0
211.6	375.0	0.5642	25.020	22.4	-385.2	7408.1802	10000	-0.09455	-2.739E-3	9260.2	9.2602E5	3.384E-3	0.4	2.4	146.020	649.07	300.0
213.8	375.0	0.5700	26.020	22.4	-391.0	7786.7100	10000	-0.09597	-2.781E-3	9733.4	9.7334E5	3.383E-3	0.4	2.5	147.020	655.80	300.0
212.6	375.0	0.5670	27.024	22.4	-405.1	8036.0801	10000	-0.09942	-2.880E-3	10045	1.0045E6	3.383E-3	0.5	2.5	148.024	652.36	300.0
212.3	375.0	0.5661	28.024	22.4	-410.0	8413.1504	10000	-0.1006	-2.916E-3	10516	1.0516E6	3.383E-3	0.5	2.5	149.024	651.30	300.0
213.6	375.0	0.5696	29.020	22.4	-409.2	8664.6104	10000	-0.1004	-2.910E-3	10831	1.0831E6	3.384E-3	0.5	2.5	150.020	655.37	300.0
211.5	375.0	0.5641	30.020	22.4	-385.2	8915.8604	10000	-0.09455	-2.739E-3	11145	1.1145E6	3.383E-3	0.5	2.5	151.020	648.98	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

208.9	372.0	0.5617	1.0040	22.4	-381.1	224.3240	10000	-0.09353	-2.754E-3	280.41	28041	3.384E-3	0.0	2.5	152.004	641.03	297.6
202.8	364.5	0.5565	2.0080	22.4	-370.3	581.3330	10000	-0.09090	-2.788E-3	726.67	72667	3.384E-3	0.0	2.6	153.008	622.25	291.6
200.6	359.4	0.5581	3.0280	22.4	-355.5	819.2950	10000	-0.08724	-2.752E-3	1024.1	1.0241E5	3.384E-3	0.1	2.6	154.028	615.32	287.5
192.6	351.7	0.5477	4.0040	22.4	-389.4	1169.8300	10000	-0.09556	-3.148E-3	1462.3	1.4623E5	3.384E-3	0.1	2.6	155.004	590.88	281.3
186.7	346.7	0.5384	5.0040	22.4	-352.2	1395.1899	10000	-0.08643	-2.930E-3	1744.0	1.7440E5	3.384E-3	0.1	2.6	156.004	572.66	277.3
179.4	339.1	0.5290	6.0800	22.4	-316.6	1733.3600	10000	-0.07771	-2.754E-3	2166.7	2.1667E5	3.384E-3	0.1	2.6	157.080	550.28	271.2
175.5	333.9	0.5256	7.0040	22.4	-348.0	1959.4500	10000	-0.08542	-3.122E-3	2449.3	2.4493E5	3.384E-3	0.1	2.6	158.004	538.32	267.1
171.9	328.8	0.5227	8.0200	22.4	-334.0	2173.2400	10000	-0.08197	-3.089E-3	2716.6	2.7166E5	3.384E-3	0.1	2.7	159.020	527.31	263.1
164.8	321.2	0.5131	9.0040	22.4	-319.1	2491.0000	10000	-0.07832	-3.092E-3	3113.8	3.1138E5	3.384E-3	0.2	2.7	160.004	505.67	257.0
159.1	316.1	0.5035	10.004	22.4	-330.7	2703.7400	10000	-0.08116	-3.310E-3	3379.7	3.3797E5	3.384E-3	0.2	2.7	161.004	488.20	252.9
153.6	308.4	0.4980	11.016	22.4	-306.7	3011.3799	10000	-0.07527	-3.225E-3	3764.2	3.7642E5	3.383E-3	0.2	2.7	162.016	471.18	246.7
152.0	303.3	0.5012	12.004	22.4	-338.1	3212.6399	10000	-0.08298	-3.675E-3	4015.8	4.0158E5	3.384E-3	0.2	2.7	163.004	466.38	242.7
147.1	298.2	0.4932	13.000	22.4	-316.6	3410.8201	10000	-0.07771	-3.561E-3	4263.5	4.2635E5	3.384E-3	0.2	2.7	164.000	451.18	238.5
142.1	290.5	0.4890	14.004	22.4	-307.5	3699.2300	10000	-0.07548	-3.643E-3	4624.0	4.6240E5	3.384E-3	0.2	2.8	165.004	435.84	232.4
135.0	285.5	0.4730	15.020	22.4	-274.4	3886.4299	10000	-0.06736	-3.367E-3	4858.0	4.8580E5	3.384E-3	0.3	2.8	166.020	414.28	228.4
129.1	277.7	0.4647	16.004	22.4	-301.7	4168.8501	10000	-0.07406	-3.911E-3	5211.1	5.2111E5	3.383E-3	0.3	2.8	167.004	395.99	222.2
125.3	272.6	0.4598	17.000	22.4	-287.7	4349.3799	10000	-0.07061	-3.872E-3	5436.7	5.4367E5	3.384E-3	0.3	2.8	168.000	384.52	218.1
122.9	265.0	0.4638	18.008	22.4	-295.9	4612.1899	10000	-0.07264	-4.214E-3	5765.2	5.7652E5	3.384E-3	0.3	2.8	169.008	377.08	212.0
118.0	259.8	0.4540	19.004	22.4	-287.7	4787.1499	10000	-0.07061	-4.261E-3	5983.9	5.9839E5	3.383E-3	0.3	2.8	170.004	361.95	207.9
113.0	254.6	0.4437	20.008	22.4	-281.1	4962.2100	10000	-0.06898	-4.337E-3	6202.8	6.2028E5	3.384E-3	0.3	2.9	171.008	346.58	203.7
107.3	247.0	0.4346	21.004	22.4	-272.8	5207.7700	10000	-0.06695	-4.473E-3	6509.7	6.5097E5	3.384E-3	0.4	2.9	172.004	329.27	197.6
103.2	241.8	0.4267	22.000	22.4	-254.6	5368.7100	10000	-0.06249	-4.354E-3	6710.9	6.7109E5	3.384E-3	0.4	2.9	173.000	316.57	193.4
97.34	234.0	0.4160	23.008	22.4	-253.8	5606.0801	10000	-0.06229	-4.635E-3	7007.6	7.0076E5	3.384E-3	0.4	2.9	174.008	298.64	187.2
94.46	229.0	0.4125	24.004	22.4	-252.1	5756.1001	10000	-0.06188	-4.809E-3	7195.1	7.1951E5	3.384E-3	0.4	2.9	175.004	289.81	183.2
91.51	223.8	0.4088	25.004	22.4	-258.7	5906.2002	10000	-0.06350	-5.164E-3	7382.8	7.3828E5	3.383E-3	0.4	2.9	176.004	280.74	179.1
86.59	215.9	0.4010	26.000	22.4	-237.2	6133.4102	10000	-0.05823	-5.088E-3	7666.8	7.6668E5	3.384E-3	0.4	3.0	177.000	265.67	172.7
83.00	210.8	0.3937	27.020	22.4	-232.3	6269.1699	10000	-0.05701	-5.226E-3	7836.5	7.8365E5	3.384E-3	0.5	3.0	178.020	254.63	168.7
76.68	203.1	0.3775	28.004	22.4	-241.4	6474.6299	10000	-0.05924	-5.850E-3	8093.3	8.0933E5	3.383E-3	0.5	3.0	179.004	235.24	162.5
74.05	197.8	0.3743	29.000	22.4	-236.4	6612.0400	10000	-0.05803	-6.041E-3	8265.1	8.2651E5	3.384E-3	0.5	3.0	180.000	227.18	158.3
70.81	192.5	0.3678	30.004	22.4	-230.6	6743.1602	10000	-0.05661	-6.223E-3	8429.0	8.4290E5	3.383E-3	0.5	3.0	181.004	217.23	154.0
65.96	184.8	0.3568	31.004	22.4	-228.2	6931.5200	10000	-0.05600	-6.678E-3	8664.4	8.6644E5	3.383E-3	0.5	3.0	182.004	202.35	147.9
63.92	179.5	0.3561	32.000	22.4	-233.1	7055.1699	10000	-0.05722	-7.232E-3	8819.0	8.8190E5	3.383E-3	0.5	3.1	183.000	196.12	143.6
60.07	174.2	0.3448	33.004	22.4	-217.4	7173.7202	10000	-0.05336	-7.163E-3	8967.2	8.9672E5	3.384E-3	0.6	3.1	184.004	184.28	139.4
55.55	166.6	0.3335	34.004	22.4	-225.7	7342.1499	10000	-0.05539	-8.134E-3	9177.7	9.1777E5	3.384E-3	0.6	3.1	185.004	170.42	133.3
53.63	161.3	0.3326	35.004	22.4	-226.5	7457.1299	10000	-0.05559	-8.709E-3	9321.4	9.3214E5	3.384E-3	0.6	3.1	186.004	164.55	129.0
50.01	155.8	0.3210	36.008	22.4	-217.4	7566.5298	10000	-0.05336	-8.958E-3	9458.2	9.4582E5	3.383E-3	0.6	3.1	187.008	153.44	124.6
46.89	148.0	0.3168	37.004	22.4	-217.4	7716.3301	10000	-0.05336	-9.923E-3	9645.4	9.6454E5	3.384E-3	0.6	3.1	188.004	143.87	118.4
43.66	142.7	0.3060	38.000	22.4	-207.5	7815.8301	10000	-0.05093	-0.01019	9769.8	9.7698E5	3.384E-3	0.6	3.2	189.000	133.95	114.2
41.02	137.2	0.2990	39.004	22.4	-200.0	7915.3501	10000	-0.04910	-0.01063	9894.2	9.8942E5	3.384E-3	0.7	3.2	190.004	125.84	109.8
37.10	129.4	0.2866	40.004	22.4	-186.0	8046.1499	10000	-0.04565	-0.01110	10058	1.0058E6	3.383E-3	0.7	3.2	191.004	113.83	103.6
34.98	124.1	0.2818	41.004	22.4	-198.4	8133.5898	10000	-0.04869	-0.01288	10167	1.0167E6	3.384E-3	0.7	3.2	192.004	107.31	99.30
31.89	118.6	0.2690	42.004	22.4	-204.2	8220.3096	10000	-0.05011	-0.01452	10275	1.0275E6	3.383E-3	0.7	3.2	193.004	97.840	94.86
29.07	110.8	0.2623	43.004	22.4	-191.0	8333.0596	10000	-0.04687	-0.01555	10416	1.0416E6	3.384E-3	0.7	3.2	194.004	89.172	88.65
26.66	105.5	0.2528	44.004	22.4	-181.9	8407.2197	10000	-0.04464	-0.01635	10509	1.0509E6	3.384E-3	0.7	3.3	195.004	81.802	84.38
24.15	99.86	0.2418	45.016	22.4	-181.9	8482.8604	10000	-0.04464	-0.01824	10604	1.0604E6	3.384E-3	0.8	3.3	196.016	74.096	79.89
21.88	94.18	0.2323	46.004	22.4	-189.3	8581.0195	10000	-0.04646	-0.02134	10726	1.0726E6	3.384E-3	0.8	3.3	197.004	67.113	75.34
19.07	86.19	0.2213	47.000	22.4	-179.4	8642.6904	10000	-0.04403	-0.02415	10803	1.0803E6	3.384E-3	0.8	3.3	198.000	58.511	68.95
16.75	80.45	0.2083	48.020	22.4	-176.1	8704.1396	10000	-0.04322	-0.02720	10880	1.0880E6	3.384E-3	0.8	3.3	199.020	51.402	64.36
14.85	74.60	0.1990	49.004	22.4	-171.1	8759.6699	10000	-0.04200	-0.03075	10950	1.0950E6	3.384E-3	0.8	3.3	200.004	45.547	59.68
12.89	69.29	0.1861	50.004	22.4	-175.3	8809.0303	10000	-0.04301	-0.03650	11011	1.1011E6	3.383E-3	0.8	3.4	201.004	39.552	55.43
11.78	63.55	0.1854	51.004	22.4	-157.9	8858.2305	10000	-0.03875	-0.03910	11073	1.1073E6	3.384E-3	0.9	3.4	202.004	36.139	50.84
9.211	55.14	0.1670	52.004	22.4	-167.8	8919.8096	10000	-0.04119	-0.05519	11150	1.1150E6	3.384E-3	0.9	3.4	203.004	28.258	44.11
8.105	49.71	0.1631	53.000	22.4	-169.5	8956.3604	10000	-0.04159	-0.06859	11195	1.1195E6	3.384E-3	0.9	3.4	204.000	24.867	39.77
6.541	43.64	0.1499	54.020	22.4	-171.9	8992.9199	10000	-0.04220	-0.09028	11241	1.1241E6	3.384E-3	0.9	3.4	205.020	20.068	34.91
4.893	37.28	0.1312	55.004	22.4	-183.5	9023.1104	10000	-0.04504	-0.1320	11279	1.1279E6	3.384E-3	0.9	3.4	206.004	15.010	29.83
3.671	31.85	0.1152	56.004	22.4	-167.0	9047.3799	10000	-0.04098	-0.1646	11309	1.1309E6	3.383E-3	0.9	3.5	207.004	11.261	25.48
2.589	25.38	0.1020	57.020	22.4	-167.0	9070.9697	10000	-0.04098	-0.2592	11339	1.1339E6	3.384E-3	1.0	3.5	208.020	7.9440	20.30
1.556	18.20	0.08550	58.004	22.4	-161.2	9088.3301	10000	-0.03956	-0.4869	11360	1.1360E6	3.383E-3	1.0	3.5	209.004	4.7727	14.56
0.8097	12.32	0.06572	59.004	22.4	-157.1	9099.6104	10000	-0.03855	-1.035	11375	1.1375E6	3.384E-3	1.0	3.5	210.004	2.4841	9.856
0.4354	8.259	0.05272	60.020	22.4	-157.1	9104.5400	10000	-0.03855	-2.303	11381	1.1381E6	3.384E-3	1.0	3.5	211.020	1.3357	6.607

